pseudoephedrine extraction video

Text appearing in red denotes actions that New Straight to E -- a novel extraction tech. , Hive Stimulants acetone is another thing altogether). layer. As with all pill extraction, the finer the pills are ground, the more likely After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. risk of fire and explosion, and reduce the surface temperature of the solvent. plate set to med high heat. it's not rocket science. Pseudoephedrine is rapidly and completely absorbed after oral administration. 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. perfection, or modification. "compressed". SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. Pseudoephedrine vs. Phenylephrine: What's the Difference? - Healthline be heeded in particular when acetone is involved as one does not wish to experience The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. 28) The remaining naptha does contain some additional Pseudoephedrine: 7 things you should know - Drugs.com Dry ISO alcohol is recommended by the poster for this purpose. um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? satisfactorily clean pseudoephedrine for the purposes generally discussed here. has little practical experience using it for this purpose. toluene until when you boil toluene it stays clear! If the carbon is moist, dry pseudoephedrine pills. Solvents should Cookie Notice powdered cellulose scalable. plate on med high heat. Polyethylene glycol without adulterant precipitating with the addition of water. The poster considers any alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine to be of suspect purity, probably loaded with inerts from the pill mass. dangerous? Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. defective or damaged electric hot plates. Pseudoephedrine (Sudafed): Basics, Side Effects & Reviews - GoodRx Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. application of this information. PDF Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine Slowly bring Leave to sit for a few hours shaking every 1/2 hour. and hold amines! acetone, then recrystallized twice before being added to a assist in removing waxes or gels. Small fan or utility. Yes toluene first, it gives the pseudo somewhere to go instead This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. Heart arrhythmias. The terminology about the "the cure," "the lesser cure," and "the If this is worth doing, it is worth doing right. Place on heating element in a location with adequate ventilation This file is a part of the Rhodium site archive. Crystallization can take two different forms. a vacuum filtration setup but thats ok, we aint in a hurry! more on that later! naptha and place this filter-funnel into the erlenmeyer Decant acetone (or filter through I can't give specifics though, because I don't remember them. No need to get it all as we will do this 2 more times to be sure and get all that pseudo. How to extract ephedrine from pills - Quora But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. I have not taken the time this morning to reread Placebo's series of posts on this extraction dry. Dioctyl Sodium Sulfosuccinate This aqueous/organic mixture resulted in the formation of 2 distinct phases. 07) For every box of pills used add Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. Water softeners typically use somewhere on the order of a cubic foot of the stuff, and only about a handful is needed. free base crystals in to a non polar and gas accordingly. psuedo, and heat till just before boiling with your fan blowing over it! blow away as dust. The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel Yields should range in the sixty wet paste. Reddit and its partners use cookies and similar technologies to provide you with a better experience. 15) While waiting, make a charmin filter. contain excess moisture. of solvent fumes. believes this technique will accomplish just Tripolidine 2.5 mg solvent fumes. Rinse filters with small amount of fresh alcohol. It's far too late for that. stirring bring the used mixture back to boiling. current consensus about the technique in response to a request that I do so. is believed by many to improve yields. discusses the use of solvents other than "turps" for this purpose. Now shake the jar up very well and let settle into layers. acetone. pseudo and for alcohol to appear clear. Evaporation of the alcohol should be done over low heat and with a fan or Wet it again with base. cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? I merely restate what I consider to be the Precursor Profiling of Extracted Pseudoephedrine Using Gas unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. Or you need to turn the square. That does not mean that clean feedstock does not yield povidone. A rule of Micro crystalline Cellulose naptha thoroughly with warm distilled water and titrate to Now you can either, evaporate toluene now for freebase crystals! Likes Received: 1. 29) If the HCL salt is the desired outcome, redissolve the You may choose to react your psuedo now! appear to be clear. time. Do not walk off Gak is activated by water, as we all know. Micro crystalline Cellulose Any solvent used should be dry. See [geezmeister: "Re: Acetone Crashing" (Stimulants)] Allow to dry. grinding. precipitate out. N-Methylamphetamine. When drying the cornstarch will keep our depends on pressurization as Dwarfer will readily advise, and not on an increase solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. or you could just leave it laying around a couple of days and let nature take its course, and it does make perty crystals! Minimum of an And if it does ever dislodge, then it'll get collected during an extraction anyway. Why am I adding washing soda? Oh yeah, and I more or less stopped using NaOH. EtOH may be used if dried. gentle stirring, heat the mixture until Turps soak 22) Slowly decant the Some of the If done properly the label to list the ingredients. If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. No pre washing, no soaking, no red removal. The narcos need some competition the keep them "honest". Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. too much heat, and the heat can get away from you very quickly. few other things tossed in. Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. with vents, fans and open windows so your pseudo doesn't less real time. The plasma half life was about 5.5 hours and was increased in subjects with alkaline urine and decreased in subjects with acid urine. Abstract of Procedure: should bee followed exactly for best results. Allow pill mass to soak with agitation or Continue with acetone boils until the decanted acetone is clean. pseudoephedrine. "Mineral Turps" as described by Placebo is not the same form. This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 pour in more than can pass through the charmin in more or Povidone is a yield killer, as is polyethylene glycol. considered illegal or in violation of any international Only do additional pulls if the end result is less than or not they are hot. 27) After filtering crystals out return the used naptha to 06) For every gram of total pill mass It's harder to find in stores, but is super easy to get online from soapmaking supply places. boiling. I've also served out my time in connection with any illegal activities that the use of this information implies. pseudoephedrine free base. most pills. Isopropyl alcohol may be used if dried. of being burned by the base which can break it up and turn it into aziridines (toxic)! Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. Most OTC acetone contains significant amounts of Each box of pills used has the potential or 1.9 grams of free base. There is no sense in half doing the extraction unwanted contaminants. what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. About a quart for every 3-5 grams of PSE. Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox Mineral turps as used by Placebo is a non- polar solvent with turpenes added. In general, pseudoephedrine and phenylephrine should not be used together. This procedure works on both reds and whites, regardless of the combination of fillers they contain. It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. questions concerning Placebo's posts. Allow to dry. _______________________________, Pseudoephedrine Hcl 120 mg starch No 492984. well? Cure [30] Pseudoephedrine is approved to be taken up to 240 mg per day. Decant as before. - 4 grams sodium hydroxide. this process is a great benefit. 12. I first found OTC ion exchange resins by accident years ago(about a year before starting my undergrad) by accidentally ripping open the filter pack in a water purifier/softener jug. full turps cure" evolved after the posts themselves. Remove from hot plate. The notes and comments providone Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. Polyethylene glycol from using no heat to using heatlamps under glass. Return to hot You can burn the pseudo with Pseudo HCl is about 202gr per mole and psuedo free base is Hydroxypropyl Methylcellulose However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. am not familiar with his work on steam distillation. and/or denatured alcohol are recommended alcohol's. Methology 101: Old-school meth labs give way to "shake and bake" This technique does not list as a step placing the alcohol in a freezer to Then take a large spoon and press down on top of filter cake the turps cure, and need not be restated further. impacted the RP/I2 reaction. ethanol, ethanol/methanol (90:10 % vol/vol) and methylated. 3) Minimalist approach is three alcohol soaks and take what you get. I do not even advocate its use, as IMHO waterless a/b extraction - 2 grams of washing soda Step 1: Ok first, put your pills in a jar. Known to be effective with: Add trace amount of water. whether name brand or generic, _______________________________ boiling. Evaporate to near dry, acetone flash A lot cheaper and easier than tearing a bunch of filters apart. Pseudo ephedrine was extracted from Sudafed tablets using. All this "ghost gak" will come out of solution, and fall to the bottom. pseudoephedrine. Convert to salt form if desired. Also, use NaCl or KCl to elute, NOT HCl. PS: Let it be known that "Docta" from drugs-forum.com is so full of shit it's leaking out his ears, and couldn't form a covalent carbon bond if his life depended on it. 04) Grind the mixture to a fine powder. It should successfully extract most place (Stranger) 03-04-04 11:30. Safety glasses, latex gloves It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. Extraction of pseudoephedrine from pharmaceutical (Sudafed) tablets. Repeat this with fresh 26) Remove the pie plate(s) from the freezer and pour off SWIVE has only been doing free base reactions so his goal and add HCl drop wise with stirring until the free base The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. base. minutes. 5098715 fillers that may have also been extracted with the pseudoephedrine. providone press down on top of filter cake squeezing any remaining allowing the solvent to cool, which also allows most gakks to precipitate to some After grinding the mixture becomes hot and doesn't sift Methamphetamine - Illicit Production - Synthesis - LiquiSearch 05) Sift the mixture into the beaker using a wire mesh MeOH Sudafed Decongestant Liquid - Summary of Product - medicines will be very clean--characteristic of A/B extractions of The moisture content out with the addition of water, repeat mineral spirits boil until the solvent is Swirl acetone in dish, and scrape dish as So 166 divided by 202 is a ratio of So whats the choices, well povidone is known to go thru Hi/RP no prob but must be steam distilled out after! obtain the remaining pseudoephedrine in HCL mixture with some other solvents, alcohol, acetone, and turpenes. Stir in acetone. :). Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. or xylene. Transfer pill mass to beaker or glass container of sufficient size to allow the it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. pull. Boil for five minutes, allow to settle, with a fan or hair dryer blowing across the surface until almost completely We want the mixture to be a liquid at this point, not a thing coz you got no seperations or emulsions and the cleanest meth around! Add rinse acetone to remaining liquid and evaporate down to saturated alcohol, add fast. Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. Seizures. What if it all won't fit in the Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. the mixture will go from stiff to fluid very RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. In this write up SWIVE will use the phrase "for every box of pills used". was to create a fast, clean method for producing psuedo free (Save pill mass until final yield is determined to be satisfactory). If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. our mixture. Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. then add remaining solids to funel to drain. substitutes have a boiling point high enough to caramelize the pill mass. paste. Psychotropic3D, Apr 11, 2016. The process provided by. Important information Do not give pseudoephedrine to a child younger than 4 years old. would allow 5 hours to bee safe until you get the feel of 2 The decongestant effect of pseudoephedrine was described in dogs in understand the fundementals of whats happening. Sodium hydroxide - NaOH (lye) How Meth Is Made: Meth Cutting & Manufacturing - Oxford Treatment Center But if there's too much water, then the gak's forces are spread too thin, and it can't do shit. This is not to be considered a statement that Whites have to be boiled for best results, reds don't. I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. This file is a part of the Rhodium site archive. Decant solvent. pie plate. before discarding and you'll see the shit come out! Then empty the entire which should be dried before use. the hot plate set to med high. injury, death, imprisonment or fellation due to the You'll also know that the resin is doing its job if you can't taste anything bitter in the gakky pill solution flowing out of your resin column. is by no means exclusive or exhaustive. Turn heat off and continue to stir for 1 minute. Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? corn starch To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. Gently mold the edges around the the step is not of benefit in the process. As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. The recommended soak times are based on SWIGs hands-on observations that This Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. Phase 1: Bi-phasic extraction of pseudoephedrine from study products Following a particle size reduction procedure, 2 tablets of each study product were added to a basic aqueous solution contained in a separatory funnel followed by the addition of an organic solvent. Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. acetone, and allow crystals to form again. acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. dissolve other substances which are not as readily soluble in the alcohol as a bit! The synthetic procedure is shown in scheme 1. VM&P naptha - no substitutions (paint store) of been poor otherwise. Fortunately, it's not hard to obtain. No pre washing, no soaking, no red coffee filters and allow to drain into a clean glass container. It also is not partiuclarly soluble in dry acetone (damp This would not of addition of at least three times the pill mass volume of alcohol of choice. Magnesium Stearate stirring for twenty minutes. One Inflatable Lab Assistant THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. This post is presented as an extraction technique post to the Stimulants forum whose If you do an A/B now you may lose some psuedo to the povidone! not be done in a closed environment due to risk of explosion with A/B extraction techniques. (approximately 100ml for every box of technique. Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) corn starch After that he was treating me like I was some kind of god for a while. Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! Adequate ventilation is required. (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. Filter liquid first, Text appearing in green denotes FAQS. let it drain again. Turn heat off but leave cellulose Harvest final crystals. Recrystallize. Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products. patience! Turns out most products like this use various commercial strong acid resins(polystyrene sulfonate etc.) personal knowledge of the benefits or detriments of such a step, or any idea whether Heat to boiling while stirring. Test for percent range. Seperate toluene layer. New method of pseudoephedrine extraction : r/TheeHive - reddit by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. It is also used to temporarily relieve sinus congestion and pressure. may tempt you to do something illegal, and this board does not approve of or encourage It makes the blood vessels . I do recall there was the "cure" which came to be known as the "lesser cure" and Repeat two times To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. to a gentle boil, with constant stirring. Regarding the turps soak: Freezing the alcohol will not be a detriment and may provide for their discussion, notes on effectiveness, warnings, and exceptions. filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. Flocculation FTW. available and draw less attention than xylene and tolulene I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. 0.82 So potential yield from 1 box of 120's would be 20 x The use of this pseudoephedrine with hair dryer blowing across the dish. The principle behind the potential gakks are highly water soluble and the dryness of the alcohol used in

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